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ChemicalBook CAS DataBase List 2,2,5,6-TETRAMETHYL-4H-1,3-DIOXIN-4-ONE

2,2,5,6-TETRAMETHYL-4H-1,3-DIOXIN-4-ONE synthesis

4synthesis methods
-

Yield:87769-39-9 71%

Reaction Conditions:

with sulfuric acid;acetic anhydride1.) ice-cooling, 3 h, 2.) 0 deg C, 12 h;

References:

Sato, Masayuki;Ogasawara, Hiromichi;Oi, Keiichi;Kato, Tetsuzo [Chemical and pharmaceutical bulletin,1983,vol. 31,# 6,p. 1896 - 1901]

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