2,2-bis-(trimethylsilyl)dithiane synthesis
2synthesis methods
- Product Name:2,2-bis-(trimethylsilyl)dithiane
- CAS Number:13411-46-6
- Molecular formula:C10H24S2Si2
- Molecular Weight:264.6
Yield:13411-46-6 90%
Reaction Conditions:
Stage #1: 1,3 dithianewith n-butyllithium in tetrahydrofuran;hexane at 0; for 0.25 h;Inert atmosphere;
Stage #2: chloro-trimethyl-silane in tetrahydrofuran;hexane at 0 - 20;Inert atmosphere;
References:
Manvar, Atul;O'Shea, Donal F. [European Journal of Organic Chemistry,2015,vol. 2015,# 33,p. 7259 - 7263] Location in patent:supporting information
