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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

2-(2-Bromo-6-fluorophenyl)nicotinonitrile synthesis

1synthesis methods
2-(2-fluorophenyl)nicotinonitrile

868944-69-8
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2-(2-Bromo-6-fluorophenyl)nicotinonitrile

1213704-92-7
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Yield:1213704-92-7 66%

Reaction Conditions:

with N-Bromosuccinimide;copper diacetate;palladium diacetate in acetonitrile at 150; for 2 h;Microwave irradiation;regioselective reaction;

References:

Cailly, Thomas;Begtrup, Mikael [Tetrahedron,2010,vol. 66,# 6,p. 1299 - 1307] Location in patent:experimental part