2-(2-BroMocyclohex-1-en-1-yl)ethan-1-ol synthesis
- Product Name:2-(2-BroMocyclohex-1-en-1-yl)ethan-1-ol
- CAS Number:85236-15-3
- Molecular formula:C8H13BrO
- Molecular Weight:205.09
83043-84-9
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85236-15-3
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Yield:85236-15-3 82%
Reaction Conditions:
Stage #1: 1-Bromo-2-ethenylcyclohex-1-enewith 9-bora-bicyclo[3.3.1]nonane in tetrahydrofuran at 20; for 26 h;Inert atmosphere;
Stage #2: with dihydrogen peroxide;sodium hydroxide in tetrahydrofuran;methanol; for 3 h;Reflux;
References:
Zhan, Fuxu;Liang, Guangxin [Angewandte Chemie - International Edition,2013,vol. 52,# 4,p. 1266 - 1269][Angew. Chem.,2012,vol. 125,# 4,p. 1304 - 1307,4] Location in patent:supporting information
38127-47-8
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85236-15-3
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108-94-1
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$12.00/50g
85236-15-3
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