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2,2-dibromodiphenylmethane synthesis

10synthesis methods
Benzenemethanol, 2-bromo-α-(2-bromophenyl)-

123335-02-4
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2,2-dibromodiphenylmethane

61592-89-0
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Yield:61592-89-0 99%

Reaction Conditions:

Stage #1: bis-(2-bromophenyl)methanolwith trifluoroacetic acid in dichloromethane at 0; for 0.0833333 h;
Stage #2: with triethylsilane in dichloromethane at 0 - 20; for 16 h;

References:

Doan, Thu-Hong;Chardon, Aurélien;Osi, Arnaud;Mahaut, Damien;Tumanov, Nikolay;Wouters, Johan;Champagne, Beno?t;Berionni, Guillaume [Chemistry - A European Journal,2021,vol. 27,# 5,p. 1736 - 1743] Location in patent:supporting information