ChemicalBook CAS DataBase List 2,2-DIMETHYL-4(S)-4-IODOMETHYL-1,3-DIOXALANE

2,2-DIMETHYL-4(S)-4-IODOMETHYL-1,3-DIOXALANE synthesis

2synthesis methods

Product Name:2,2-DIMETHYL-4(S)-4-IODOMETHYL-1,3-DIOXALANE
CAS Number:23735-44-6
Molecular formula:C6H11IO2
Molecular Weight:242.05

14347-78-5 Synthesis

(R)-(-)-2,2-Dimethyl-1,3-dioxolane-4-methanol

14347-78-5
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2,2-DIMETHYL-4(S)-4-IODOMETHYL-1,3-DIOXALANE

23735-44-6
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Yield:23735-44-6 90%

Reaction Conditions:

with 1H-imidazole;iodine;triphenylphosphine in toluene at 90; for 2 h;

References:

Liu, Yonghui;Yan, Bocheng;Wang, Zhaoyu;Zhu, Haomiao;Yin, Xiaona;Wang, Kun;Wang, Menglei;Zhao, Wei [ACS Medicinal Chemistry Letters,2020,vol. 11,# 7,p. 1371 - 1376] Location in patent:supporting information

23735-43-5 Synthesis

(S)-2,2-Dimethyl-1,3-dioxolane-4-methanol p-toluenesulfonate

23735-43-5
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$20.00/250mg

23735-44-6
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References