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ChemicalBook CAS DataBase List 2,2-DIMETHYL-4(S)-4-IODOMETHYL-1,3-DIOXALANE
23735-44-6

2,2-DIMETHYL-4(S)-4-IODOMETHYL-1,3-DIOXALANE synthesis

2synthesis methods
14347-78-5 Synthesis
(R)-(-)-2,2-Dimethyl-1,3-dioxolane-4-methanol

14347-78-5
346 suppliers
$6.00/1g

2,2-DIMETHYL-4(S)-4-IODOMETHYL-1,3-DIOXALANE

23735-44-6
8 suppliers
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Yield:23735-44-6 90%

Reaction Conditions:

with 1H-imidazole;iodine;triphenylphosphine in toluene at 90; for 2 h;

References:

Liu, Yonghui;Yan, Bocheng;Wang, Zhaoyu;Zhu, Haomiao;Yin, Xiaona;Wang, Kun;Wang, Menglei;Zhao, Wei [ACS Medicinal Chemistry Letters,2020,vol. 11,# 7,p. 1371 - 1376] Location in patent:supporting information