2,2-diMethyl-5-propanoyl-1,3-dioxane-4,6-dione synthesis
2synthesis methods
- Product Name:2,2-diMethyl-5-propanoyl-1,3-dioxane-4,6-dione
- CAS Number:64074-05-1
- Molecular formula:C9H12O5
- Molecular Weight:200.19
Yield:64074-05-1 92%
Reaction Conditions:
with pyridine in dichloromethane at 0 - 20; for 21 h;
References:
Mo, Sangjoon;Kim, Dong Hwan;Lee, Jong Hyun;Park, Je Won;Basnet, Devi B.;Ban, Yeon Hee;Yoo, Young Ji;Chen, Shu-Wei;Park, Sung Ryeol;Choi, Eun Ae;Kim, Eunji;Jin, Ying-Yu;Lee, Sung-Kwon;Park, Ju Yeol;Liu, Yuan;Lee, Mi Ok;Lee, Keum Soon;Kim, Sang Jun;Kim, Dooil;Park, Byoung Chul;Lee, Sang-Gi;Kwon, Ho Jeong;Suh, Joo-Won;Moore, Bradley S.;Lim, Si-Kyu;Yoon, Yeo Joon [Journal of the American Chemical Society,2011,vol. 133,# 4,p. 976 - 985] Location in patent:supporting information; experimental part
