![265994-70-5](/CAS/20150408/GIF/265994-70-5.gif)
2,2-dimethyl-6-nitro-2H-1,4-benzothiazin-3(4H)-one synthesis
- Product Name:2,2-dimethyl-6-nitro-2H-1,4-benzothiazin-3(4H)-one
- CAS Number:265994-70-5
- Molecular formula:C10H10N2O3S
- Molecular Weight:238.26
![Benzenethiol,2,4-dinitro-](/CAS/20180531/GIF/2218-96-4.gif)
2218-96-4
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![2,2-dimethyl-6-nitro-2H-1,4-benzothiazin-3(4H)-one](/CAS/20150408/GIF/265994-70-5.gif)
265994-70-5
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$90.00/1mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: 75 percent / K2CO3 / dimethylformamide / 7 h / 50 °C
2: 84 percent / Fe powder; 1N HCl / ethanol; H2O / 2 h / Heating
3: 85 percent / 1N NaOH / 0.5 h / Heating
4: 28 percent / conc. H2SO4; NaNO2; CuSO4 / H2O / 1 h / 0 °C
References:
Matsumoto, Yuzo;Tsuzuki, Ryuji;Matsuhisa, Akira;Yoden, Toru;Yamagiwa, Yoko;Yanagisawa, Isao;Shibanuma, Tadao;Nohira, Hiroyuki [Bioorganic and Medicinal Chemistry,2000,vol. 8,# 2,p. 393 - 404]
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369-36-8
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![2-MERCAPTOISOBUTYRIC ACID](/CAS/GIF/4695-31-2.gif)
4695-31-2
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![2,2-dimethyl-6-nitro-2H-1,4-benzothiazin-3(4H)-one](/CAS/20150408/GIF/265994-70-5.gif)
265994-70-5
9 suppliers
$90.00/1mg