2-(2-HEXYLOXYETHOXY)ETHANOL synthesis
2synthesis methods
- Product Name:2-(2-HEXYLOXYETHOXY)ETHANOL
- CAS Number:5274-61-3
- Molecular formula:C20H42O3
- Molecular Weight:330.55
Yield:-
Steps:
2 2-(2-Hexadecyloxyethoxy)ethanol
PREPARATION 2 2-(2-Hexadecyloxyethoxy)ethanol Following the procedure described in preparation 1, but using 1-bromohexadecane instead of 1-bromooctadecane, the title compound was obtained as an oil in a similar yield. IR (film)νmax (cm-1): 3350, 2910, 1489, 1467, 1320, 1143, 1078; 1 H NMR (80 MHz, CDCl3)δ ppm (TMS): 3.9-3.6 (m, 8H, OCH2 CH2 OCH2 CH2 O), 3.48 (t,J=6.3 Hz, 2H, RCH2 O), 1.7-0.7 (m, 31H aprox.). Analysis calcd. for C20 H42 O3: C 72.67%; H 12.81%. Found: C 72.88%; H 13.02%.
References:
J. Uriach & Cia US5134151, 1992, A