2-(2-Methoxyphenoxy)ethylamine synthesis
- Product Name:2-(2-Methoxyphenoxy)ethylamine
- CAS Number:1836-62-0
- Molecular formula:C9H13NO2
- Molecular Weight:167.21
64464-07-9
293 suppliers
$5.00/1g
1836-62-0
312 suppliers
$6.00/10g
Yield:1836-62-0 97%
Reaction Conditions:
with sodium hydroxide in water; pH=12 - 14 at 0;
Steps:
1
To a solution of 2-(2-methoxyphenoxy) ethylamine hydrochloride (100 g) in water (200 mL), was added 10% aqueous NaOH at 00C till the pH of the solution is 12-14 and then extracted into dichloromethane (3 x 100 mL). The organic layer was washed with brine (2 X 100 mL). The organic layer was dried over Na2SO4 and concentrated to obtain 2-(2-methoxyphenoxy) ethylamine (97%).
References:
INOGENT LABORATORIES PRIVATE LIMITED1 WO2009/157015, 2009, A2 Location in patent:Page/Page column 6
![2-[2-(2-METHOXY-PHENOXY)-ETHYL]-ISOINDOLE-1,3-DIONE](/CAS/GIF/26646-63-9.gif)
26646-63-9
46 suppliers
inquiry
1836-62-0
312 suppliers
$6.00/10g
183427-87-4
38 suppliers
$15.00/5mg
1836-62-0
312 suppliers
$6.00/10g
90-05-1
743 suppliers
$5.00/1g
1836-62-0
312 suppliers
$6.00/10g
136918-14-4
0 suppliers
inquiry
53815-60-4
38 suppliers
$340.00/1g
1836-62-0
312 suppliers
$6.00/10g