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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
197-69-3

2,3-[1,3]Butadienobenzo[b]perylene synthesis

8synthesis methods
2-Bromobenzaldehyde

6630-33-7
419 suppliers
$9.00/10g

2,3-[1,3]Butadienobenzo[b]perylene

197-69-3
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-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: potassium tert-butylate / tetrahydrofuran
2: iodine / cyclohexane / Irradiation
3: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; methanol; water / 16 h / Reflux; Inert atmosphere
4: sulfuric acid; tin(II) chloride dihdyrate / dichloromethane; isopropyl alcohol / 18 h / 20 °C / Darkness

References:

Feofanov, Mikhail;Akhmetov, Vladimir;Sharapa, Dmitry I.;Amsharov, Konstantin [Organic Letters,2020,vol. 22,# 5,p. 1698 - 1702]

9-phenanthren-9-ylphenanthrene

20532-03-0
2 suppliers
$144.00/1ea

2,3-[1,3]Butadienobenzo[b]perylene

197-69-3
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References
573-17-1 Synthesis
9-Bromophenanthrene

573-17-1
322 suppliers
$6.00/5g

2,3-[1,3]Butadienobenzo[b]perylene

197-69-3
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References
Benzene, 1,1'-(1,2-ethenediyl)bis[2-bromo-

108474-32-4
0 suppliers
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2,3-[1,3]Butadienobenzo[b]perylene

197-69-3
1 suppliers
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References
1,8-Dibromophenanthrene

20342-96-5
6 suppliers
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2,3-[1,3]Butadienobenzo[b]perylene

197-69-3
1 suppliers
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References