ChemicalBook CAS DataBase List 2,3,4,5,6,7-Hexahydro-1H-indene-1-one

2,3,4,5,6,7-Hexahydro-1H-indene-1-one synthesis

4synthesis methods

Product Name:2,3,4,5,6,7-Hexahydro-1H-indene-1-one
CAS Number:22118-00-9
Molecular formula:C9H12O
Molecular Weight:136.19

38127-47-8
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22118-00-9
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Yield:-

Steps:

Multi-step reaction with 5 steps
1: 85 percent / CuI; diethylamine / Pd(PPh₃)2Cl₂ / toluene / 12 h / 28 °C
2: 82 percent / NaBH₄ / methanol / 0.5 h / 0 °C
3: 89 percent / imidazole / dimethylformamide / 5 h / 0 °C
4: 93 percent / K₂CO₃; MeOH / CH₂Cl₂ / 25 °C
5: 63 percent / TpRuPPh₃(MeCN)2SbF₆ / toluene / 20 h / 105 °C

References:

Odedra, Arjan;Datta, Swarup;Liu, Rai-Shung [Journal of Organic Chemistry,2007,vol. 72,# 9,p. 3289 - 3292]

201230-82-2 Synthesis

201230-82-2
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83043-84-9
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22118-00-9
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References

1030023-37-0
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22118-00-9
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References

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699-61-6
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22118-00-9
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References