2,3,4,5,6-PENTAKISTRIFLUOROMETHYLPHENOL synthesis
- Product Name:2,3,4,5,6-PENTAKISTRIFLUOROMETHYLPHENOL
- CAS Number:723294-91-5
- Molecular formula:C11HF15O
- Molecular Weight:434.1
608-74-2
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81290-20-2
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$13.00/1g
2340-93-4
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723294-91-5
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53812-60-5
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Yield:2340-93-4 45% ,723294-91-5 20% ,53812-60-5 14%
Reaction Conditions:
Stage #1: (trifluoromethyl)trimethylsilanewith 1,3-dimethyl-2-imidazolidinone;potassium fluoride;copper(I) bromide in N,N-dimethyl-formamide at 0;
Stage #2: hexaiodobenzene in N,N-dimethyl-formamide at 0 - 20; for 24 h;Further stages.;
References:
Kuett, Agnes;Movchun, Valeria;Rodima, Toomas;Dansauer, Timo;Rusanov, Eduard B.;Leito, Ivo;Kaljurand, Ivari;Koppel, Juta;Pihl, Viljar;Koppel, Ivar;Ovsjannikov, Gea;Toom, Lauri;Mishima, Masaaki;Medebielle, Maurice;Lork, Enno;Roeschenthaler, Gerd-Volker;Koppel, Ilmar A.;Kolomeitsev, Alexander A. [Journal of Organic Chemistry,2008,vol. 73,# 7,p. 2607 - 2620]
1018330-39-6
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723294-91-5
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