ChemicalBook CAS DataBase List 2-(3-CHLOROPROPYL)-2,5,5-TRIMETHYL-[1,3]-DIOXANE

2-(3-CHLOROPROPYL)-2,5,5-TRIMETHYL-[1,3]-DIOXANE synthesis

2synthesis methods

Product Name:2-(3-CHLOROPROPYL)-2,5,5-TRIMETHYL-[1,3]-DIOXANE
CAS Number:88128-57-8
Molecular formula:C10H19ClO2
Molecular Weight:206.71

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
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2-(3-CHLOROPROPYL)-2,5,5-TRIMETHYL-[1,3]-DIOXANE

88128-57-8
68 suppliers
$250.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 96.2 percent / 10percent HCl / tetrahydrofuran / 1 h
2: 2.) 4-Angstroem molecular sieves / 1.) p-toluenesulfonic acid / 1.) benzene, 6 h, reflux, 2.) benzene, 2 h, reflux

References:

Ryckman,D.M.;Stevens,R.V. [Journal of the American Chemical Society,1987,vol. 109,p. 4940]

5891-21-4 Synthesis

5891-21-4
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126-30-7 Synthesis

126-30-7
610 suppliers
$8.00/100g

88128-57-8
68 suppliers
$250.00/1g

References