![](/CAS/GIF/886497-51-4.gif)
2,3-DICHLORO-6-FLUOROBENZYL BROMIDE synthesis
- Product Name:2,3-DICHLORO-6-FLUOROBENZYL BROMIDE
- CAS Number:886497-51-4
- Molecular formula:C7H4BrCl2F
- Molecular Weight:257.91
![2,3-DICHLORO-6-FLUOROBENZYL ALCOHOL](/StructureFile/ChemBookStructure7/GIF/CB6208208.gif)
886497-48-9
19 suppliers
$59.00/1g
![2,3-DICHLORO-6-FLUOROBENZYL BROMIDE](/CAS/GIF/886497-51-4.gif)
886497-51-4
28 suppliers
$73.00/1g
Yield:-
Reaction Conditions:
with hydrogen bromide;acetic acid at 80; for 0.166667 h;
Steps:
2.a
a) 1 ,2-Dichloro-4-fluoro-3-(bromomethyl)benzene; 2,3-Dichloro-6-fluorophenyl)methanol (14.2 g) was dissolved in a solution of hydrogen bromide in acetic acid (140 mL) and the mixture was heated at 80 0C for 10 minutes. LC/MS showed that all of the starting material had been consumed and a new peak, corresponding to the required benzyl bromide, was visible; retention time 2.58 minutes on standard gradient. The reaction mixture was allowed to cool to room temperature.
References:
WO2006/62477,2006,A1 Location in patent:Page/Page column 5