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ChemicalBook CAS DataBase List 2,3-Dichlorophenylacetonitrile
3218-45-9

2,3-Dichlorophenylacetonitrile synthesis

10synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: sulfuric acid / Heating / reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C
2.2: 20 °C
3.1: triethylamine / dichloromethane / 0 - 20 °C
4.1: ethanol; water / 2 h / Heating / reflux

References:

Emonds-Alt, Xavier;Proietto, Vincenzo US2004/180890, 2004, A1

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