2,3-dihydro-1-Methyl-1H-Indole-5-carbonitrile synthesis
- Product Name:2,3-dihydro-1-Methyl-1H-Indole-5-carbonitrile
- CAS Number:57413-40-8
- Molecular formula:C10H10N2
- Molecular Weight:158.2
10282-33-4
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: BF3*OEt2 / xylene / 2 h / 145 °C
2.1: selenenyl bromide resin; SnCl4 / CH2Cl2 / 1 h / 0 °C
2.2: n-Bu3SnH; AIBN / toluene / 2 h / 90 °C
References:
Nicolaou;Roecker;Hughes, Robert;Van Summeren, Ruben;Pfefferkorn, Jeffrey A.;Winssinger, Nicolas [Bioorganic and Medicinal Chemistry,2003,vol. 11,# 3,p. 465 - 476]
267002-58-4
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57413-40-8
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873-74-5
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$9.00/1g
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