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2,3-O-Isopropylidene-D-lyxono-1,4-lactone synthesis

15synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: periodic acid / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
2: acetic acid; sodium cyanoborohydride / 2 h / 20 °C / Cooling with ice

References:

Moreaux, Maxime;Bonneau, Guillaume;Peru, Aurélien;Brunissen, Fanny;Janvier, Marine;Haudrechy, Arnaud;Allais, Florent [European Journal of Organic Chemistry,2019,vol. 2019,# 7,p. 1600 - 1604]