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2(3H)-Benzothiazolethione,5-hydroxy-(9CI) synthesis

1synthesis methods
55690-60-3 Synthesis
2-MERCAPTO-5-METHOXYBENZOTHIAZOLE

55690-60-3
67 suppliers
$18.00/100mg

2(3H)-Benzothiazolethione,5-hydroxy-(9CI)

89677-89-4
4 suppliers
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Yield:89677-89-4 63%

Reaction Conditions:

with aluminum (III) chloride in toluene; for 3 h;Inert atmosphere;Reflux;

References:

Toda, Narihiro;Asano, Shigehiro;Barbas, Carlos F. [Angewandte Chemie - International Edition,2013,vol. 52,# 48,p. 12592 - 12596][Angew. Chem.,2013,vol. 125,# 48,p. 12824 - 12828,5] Location in patent:supporting information