2,4,6-tribromo-3,5-difluorobenzonitrile synthesis
- Product Name:2,4,6-tribromo-3,5-difluorobenzonitrile
- CAS Number:943528-40-3
- Molecular formula:C7Br3F2N
- Molecular Weight:375.79
64248-63-1
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Yield:943528-40-3 40%
Reaction Conditions:
with carbon tetrabromide;lithium tert-butoxide in N,N-dimethyl-formamide;m-xylene at 60; for 2 h;Inert atmosphere;
References:
Do, Hien-Quang;Daugulis, Olafs [Organic Letters,2009,vol. 11,# 2,p. 421 - 423] Location in patent:supporting information; experimental part Popov, Ilya;Do, Hien-Quang;Daugulis, Olafs [Journal of Organic Chemistry,2009,vol. 74,# 21,p. 8309 - 8313] Location in patent:supporting information; experimental part