Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 2,4,6-TRIHYDROXY PHENYL BENZYL KETONE

2,4,6-TRIHYDROXY PHENYL BENZYL KETONE synthesis

7synthesis methods
Preparation by reaction of phenylacetonitrile with phloroglucinol (Hoesch reaction),
? in the presence of boron trifluoride etherate (50%).
-

Yield:727-71-9 72.5%

Reaction Conditions:

Stage #1: 3,5-dihydroxyphenol;phenylacetonitrilewith hydrogenchloride;zinc(II) chloride in diethyl ether at 0 - 20;
Stage #2: with water in methanol; for 5 h;Reflux;

References:

Ng, Lean-Teik;Ko, Horng-Huey;Lu, Tzy-Ming [Bioorganic and Medicinal Chemistry,2009,vol. 17,# 13,p. 4360 - 4366] Location in patent:experimental part

2,4,6-TRIHYDROXY PHENYL BENZYL KETONE Related Search: