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2-(4-BROMO-PHENYL)-1H-IMIDAZOLE synthesis
- Product Name:2-(4-BROMO-PHENYL)-1H-IMIDAZOLE
- CAS Number:176961-53-8
- Molecular formula:C9H7BrN2
- Molecular Weight:223.07
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176961-53-8
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$35.00/1g
Yield: 92%
Reaction Conditions:
with tribromide-modified silica-coated magnetic nanoparticles (Fe3O4/SiO2/(CH2)3N+Me3Br3) in neat (no solvent) at 80; for 0.2 h;Green chemistry;
Steps:
2.3. General procedure for the synthesis of imidazole, benzimidazole, benzothiazole, and perimidine derivatives
General procedure: A stirred solution of the substrate (1 mmol), aryl adehyde (1 mmol),and tribromide-modified silica-coated magnetic nanoparticles (Fe3O4/SiO2/(CH2)3N+Me3Br3-, 0.007 g) was heated 80 °C. After completion of the reaction [TLC (AcOEt/hexane 1:3) monitoring], EtOH (10 mL) was added. The catalyst was recovered by an external magnet, and thereaction mixture was poured into ice-water (30 mL). The solid productwas filtered, washed with ice-water, and dried.
References:
Farrokhi, Azita;Ghodrati, Keivan;Yavari, Issa [Catalysis Communications,2015,vol. 63,p. 41 - 46]
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84 suppliers
$35.00/1g