2-(4-bromophenyl)benzo[d]oxazole synthesis
- Product Name:2-(4-bromophenyl)benzo[d]oxazole
- CAS Number:3164-13-4
- Molecular formula:C13H8BrNO
- Molecular Weight:274.11
1122-91-4
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95-55-6
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3164-13-4
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$16.00/250mg
Yield:3164-13-4 98%
Reaction Conditions:
with Amino glucose-functionalized silica-coated NiFe2O4 nanoparticles at 20; for 0.133333 h;
Steps:
2.8. General procedure for preparation of benzo[d]oxazoles 8a-kand 9a-d
General procedure: A mixture of aldehyde 1 (1.0 mmol), 1,2-aminophenol (1 mmol)and 0.05 g of NiFe2O4(at)SiO2(at)aminoglucose were stirred at roomtemperature under solvent free condition for the required reactiontime according to Table 6 and 7 After completion of the reaction, asindicated by TLC (TLC Silica gel 60 F, ethyl acetate: n-hexane 1: 4),the resulting mixture was diluted with hot ethanol (10 mL) and thecatalyst separated by the external magnet and washed with hotdistilledwater (5 mL) and ethanol (3 mL) two times. The filtratewascooled down to room temperature and the precipitated crudeproduct was recrystallized from ethanol if necessary.
References:
Fekri, Leila Zare;Nikpassand, Mohammad;Shariati, Shahab;Aghazadeh, Behnaz;Zarkeshvari, Reza;Norouz pour, Nahid [Journal of Organometallic Chemistry,2018,vol. 871,p. 60 - 73]
586-75-4
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615-36-1
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3164-13-4
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$16.00/250mg
586-76-5
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95-55-6
558 suppliers
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3164-13-4
155 suppliers
$16.00/250mg
201230-82-2
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589-87-7
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95-55-6
558 suppliers
$5.00/5G
3164-13-4
155 suppliers
$16.00/250mg
95-55-6
558 suppliers
$5.00/5G
589-17-3
156 suppliers
$10.00/5g
3164-13-4
155 suppliers
$16.00/250mg