ChemicalBook CAS DataBase List 2-(4-broMobenzyl)propanoic acid

2-(4-broMobenzyl)propanoic acid synthesis

4synthesis methods

Product Name:2-(4-broMobenzyl)propanoic acid
CAS Number:66735-01-1
Molecular formula:C10H11BrO2
Molecular Weight:243

1643-30-7 Synthesis

1643-30-7
247 suppliers
$6.00/1g

74-88-4
341 suppliers
$15.00/10g

66735-01-1
33 suppliers
$45.00/25mg

Yield:66735-01-1 54 %

Reaction Conditions:

Stage #1: 3-(4-bromophenyl)propionic acidwith n-butyllithium;diisopropylamine in tetrahydrofuran at -78 - 40;Inert atmosphere;
Stage #2: methyl iodide in tetrahydrofuran at 0 - 20;

References:

Dong, Zi-Yu;Zhao, Jia-Hui;Wang, Peng;Yu, Jin-Quan [Organic Letters,2022,vol. 24,# 42,p. 7732 - 7736] Location in patent:supporting information

diethyl 2-(4-bromobenzyl)-2-methylmalonate

70146-85-9
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inquiry

66735-01-1
33 suppliers
$45.00/25mg

References

802294-64-0 Synthesis

802294-64-0
1 suppliers
inquiry

589-15-1
434 suppliers
$6.00/10g

66735-01-1
33 suppliers
$45.00/25mg

References

2-Propenoic acid, 3-(4-bromophenyl)-2-methyl-

66735-14-6
1 suppliers
inquiry

66735-01-1
33 suppliers
$45.00/25mg

References