ChemicalBook CAS DataBase List 2-(4-broMophenyl)-1-(pyrrolidin-1-yl)ethanone

2-(4-broMophenyl)-1-(pyrrolidin-1-yl)ethanone synthesis

4synthesis methods

Product Name:2-(4-broMophenyl)-1-(pyrrolidin-1-yl)ethanone
CAS Number:13734-66-2
Molecular formula:C12H14BrNO
Molecular Weight:268.15

4030-18-6 Synthesis

4030-18-6
67 suppliers
$31.00/1g

2-(4-broMophenyl)-1-(pyrrolidin-1-yl)ethanone

13734-66-2
12 suppliers
$204.00/1g

Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium hexamethyldisilazane / tetrahydrofuran; toluene / 1 h / 0 - 5 °C / Inert atmosphere; Sealed tube
2: 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; bis(dibenzylideneacetone)-palladium⁽⁰⁾ / tetrahydrofuran; toluene / 5 h / 65 °C / Inert atmosphere; Sealed tube

References:

Wong, Brian;Linghu, Xin;Crawford, James J.;Drobnick, Joy;Lee, Wendy;Zhang, Haiming [Tetrahedron,2014,vol. 70,# 7,p. 1508 - 1515]

123-75-1 Synthesis