4-(Hexadecyloxy)benzene-1,3-diamine synthesis
- Product Name:4-(Hexadecyloxy)benzene-1,3-diamine
- CAS Number:137819-03-5
- Molecular formula:C22H40N2O
- Molecular Weight:348.57
42579-93-1
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Yield:137819-03-5 93.5%
Reaction Conditions:
with hydrogen in ethanol at 60; under 30003 Torr; for 2 h;Autoclave;Temperature;
Steps:
2
Then, 1,3-dinitro-4-hexadecyloxybenzene was added to the autoclave, 100 ml of ethanol, 4 g of nickel, and hydrogen were pressurized to 4 MPa. The mixture was heated to 60° C., and the reaction was incubated for 2 h.1,3-Diamino-4-hexadecyloxybenzene was obtained, and the yield was 93.5%.
References:
CN108003043,2018,A Location in patent:Paragraph 0038; 0039; 0041; 0044; 0047
51-28-5
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544-77-4
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$32.79/25g
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