2,4-Dibromo-6-methylbenzoic acid synthesis
- Product Name:2,4-Dibromo-6-methylbenzoic acid
- CAS Number:58707-03-2
- Molecular formula:C8H6Br2O2
- Molecular Weight:293.94
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Yield:-
Reaction Conditions:
Stage #1: methyl-1,2,5-tribromobenzenewith isopropylmagnesium chloride in tetrahydrofuran at -40; for 2 h;Grignard reaction;
Stage #2: carbon dioxide in tetrahydrofuran at -40; for 1 h;Further stages. Title compound not separated from byproducts.;
References:
Menzel, Karsten;Mills, Paul M.;Frantz, Doug E.;Nelson, Todd D.;Kress, Michael H. [Tetrahedron Letters,2008,vol. 49,# 3,p. 415 - 418]