2’,4’-Dimethoxy-2-hydroxyacetophenone synthesis
- Product Name:2’,4’-Dimethoxy-2-hydroxyacetophenone
- CAS Number:871878-99-8
- Molecular formula:C10H12O4
- Molecular Weight:196.2
829-20-9
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: sodium hydride / tetrahydrofuran / 2.5 h / -78 - 85 °C / Inert atmosphere; Green chemistry
2: 2,2,2-Trifluoroacetophenone; dihydrogen peroxide / acetonitrile; tert-butyl alcohol / 1 h / 20 °C / Green chemistry
3: toluene-4-sulfonic acid / 1 h / 20 °C / Green chemistry
References:
Voutyritsa, Errika;Theodorou, Alexis;Kokotos, Christoforos G. [Organic and Biomolecular Chemistry,2016,vol. 14,# 24,p. 5708 - 5713]
60965-26-6
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