ChemicalBook CAS DataBase List 2,4-DIMETHYL-A-CARBOLINE

2,4-DIMETHYL-A-CARBOLINE synthesis

1synthesis methods

Product Name:2,4-DIMETHYL-A-CARBOLINE
CAS Number:13315-71-4
Molecular formula:C13H12N2
Molecular Weight:196.25

tert-Butyl 3-acetyl-1H-indole-1-carboxylate

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Yield:-

Steps:

Multi-step reaction with 2 steps
1: n-butyllithium / tetrahydrofuran; hexane / 0 - 20 °C
2: 1,2-dichloro-benzene / 3 h / 240 °C / Sealed tube; Microwave irradiation

References:

Markey, Sophie J.;Lewis, William;Moody, Christopher J. [Organic Letters,2013,vol. 15,# 24,p. 6306 - 6308]

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