![](/CAS/GIF/51163-29-2.gif)
2,4-DIMETHYLPHENYL ISOCYANATE synthesis
- Product Name:2,4-DIMETHYLPHENYL ISOCYANATE
- CAS Number:51163-29-2
- Molecular formula:C9H9NO
- Molecular Weight:147.17
![Triphosgene](/CAS/GIF/32315-10-9.gif)
32315-10-9
411 suppliers
$10.00/1g
![2,4-Dimethyl aniline](/CAS/GIF/95-68-1.gif)
95-68-1
313 suppliers
$14.00/5g
![2,4-DIMETHYLPHENYL ISOCYANATE](/CAS/GIF/51163-29-2.gif)
51163-29-2
40 suppliers
$22.60/1g
Yield:-
Reaction Conditions:
in 1,4-dioxane;Reflux;
Steps:
3.4. General Procedure for Preparation of Aromatic Isocyanates (6a-n)
General procedure: Appropriate aromatic amine (0.02 mol) was added slowly to a stirred solution of BTC (3.0 g,0.01 mol) in 1,4-dioxane (30 mL) at room temperature. After refluxing for 8-12 h, excess 1,4-dioxanewas evaporated. The residue was distilled under reduced pressure to afford compounds 6a-n.
References:
Jiang, Nan;Bu, Yanxin;Wang, Yu;Nie, Minhua;Zhang, Dajun;Zhai, Xin [Molecules,2016,vol. 21,# 11,art. no. 1572]
![2,4-DIMETHYLPHENYLUREA](/CAS/GIF/2990-02-5.gif)
2990-02-5
37 suppliers
$16.69/5g
![2,4-DIMETHYLPHENYL ISOCYANATE](/CAS/GIF/51163-29-2.gif)
51163-29-2
40 suppliers
$22.60/1g
![ETHYL N-(2,4-XYLYL)CARBAMATE](/CAS/20180703/GIF/35601-95-7.gif)
35601-95-7
5 suppliers
$28.60/250mg
![2,4-DIMETHYLPHENYL ISOCYANATE](/CAS/GIF/51163-29-2.gif)
51163-29-2
40 suppliers
$22.60/1g