2-(4-Iodophenyl)-5,5-dimethyl-1,3,2-dioxaborinane synthesis
- Product Name:2-(4-Iodophenyl)-5,5-dimethyl-1,3,2-dioxaborinane
- CAS Number:5572-94-1
- Molecular formula:C11H14BIO2
- Molecular Weight:315.94
5122-99-6
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Yield:5572-94-1 86%
Reaction Conditions:
with magnesium sulfate in dichloromethane at 20;Product distribution / selectivity;
Steps:
3.A
Method 3; 4-((4-(5,5-dimethyl-l,3,2-dioxaborinan-2-yl)phenyl)ethynyl)benzaldehyde; A. 2-(4-iodophenyl)-5,5-dimethyl-l ,3,2-dioxaborinane; 2-(4-iodophenyl)-5,5-dimethyl-l,3,2-dioxaborinane was prepared following the method described in Method 2 step A to yield 5.4 g (86% yield) of the title compound as an off-white solid.LC-MS: [M+H]+ 316.12 Mass: calculated for C11H14BIO2, 315.95
References:
WO2010/100475,2010,A1 Location in patent:Page/Page column 48
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