2-(4-METHOXY-PHENYL)-SUCCINIC ACID synthesis
- Product Name:2-(4-METHOXY-PHENYL)-SUCCINIC ACID
- CAS Number:6331-59-5
- Molecular formula:C11H12O5
- Molecular Weight:224.21
201230-82-2
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Yield:6331-59-5 85%
Reaction Conditions:
with (R,R,R,R)-Wingphos;lithium hydroxide monohydrate;palladium (II) 2,4-pentanedionate;2-(2,8-dimethyl-10H-phenoxaphosphinin-10-yl)pyridine;toluene-4-sulfonic acid in 1,2-dichloro-ethane at 70; under 22502.3 Torr; for 24 h;Autoclave;Inert atmosphere;enantioselective reaction;
References:
Ji, Xiaolei;Shen, Chaoren;Tian, Xinxin;Zhang, Hongru;Ren, Xinyi;Dong, Kaiwu [Angewandte Chemie - International Edition,2022,vol. 61,# 29,art. no. E202204156][Angew. Chem.,2022,vol. 134,# 29] Location in patent:supporting information