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2-(4-NITROPHENYL)ACETOHYDRAZIDE synthesis

5synthesis methods
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Yield:6144-81-6 93%

Reaction Conditions:

Stage #1: ethanol;4-nitrobenzeneacetic acidwith thionyl chloride at 20;
Stage #2: with hydrazine hydrate in ethanol;water at 80; for 0.75 h;

References:

Elsinghorst, Paul W.;Haertig, Wolfgang;Goldhammer, Simone;Grosche, Jens;Guetschow, Michael [Organic and Biomolecular Chemistry,2009,vol. 7,# 19,p. 3940 - 3946] Location in patent:supporting information; experimental part

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