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2,5-bis(heptyloxy)benzene-1,4-dialdehyde synthesis

2synthesis methods
14753-51-6 Synthesis
2,5-DIBROMOHYDROQUINONE

14753-51-6
201 suppliers
$6.00/1g

2,5-bis(heptyloxy)benzene-1,4-dialdehyde

206762-48-3
28 suppliers
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Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C / Inert atmosphere
2.1: n-butyllithium / diethyl ether; hexane / 2 h / 0 °C / Inert atmosphere
2.2: 18 h / 0 - 20 °C / Inert atmosphere

References:

Capomolla, Simona S.;Manfroni, Giacomo;Prescimone, Alessandro;Constable, Edwin C.;Housecroft, Catherine E. [Polyhedron,2022,vol. 224,art. no. 116005]

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