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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

2,5-Bis(triethoxysilyl)thiophene synthesis

1synthesis methods
3141-27-3 Synthesis
2,5-Dibromothiophene

3141-27-3
308 suppliers
$5.00/10g

78-10-4 Synthesis
Tetraethyl orthosilicate

78-10-4
422 suppliers
$12.00/25g

2,5-Bis(triethoxysilyl)thiophene

40190-22-5
24 suppliers
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Yield:40190-22-5 62%

Reaction Conditions:

with magnesium;ethylene dibromide in tetrahydrofuran at 20; for 0.5 h;Irradiation;sonication;sonochemical Barbier-type reaction;

References:

Lee, Adam Shih-Yuan;Chang, Yu-Ting;Chu, Shu-Fang;Tsao, Kuo-Wei [Tetrahedron Letters,2006,vol. 47,# 39,p. 7085 - 7087]