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2-(5-Chloro-2-thienyl)-5-methylpyridine synthesis

1synthesis methods
2873-18-9 Synthesis
2-BROMO-5-CHLOROTHIOPHENE

2873-18-9
182 suppliers
$8.00/1g

257876-05-4 Synthesis
5-METHYL-2-PYRIDYLZINC BROMIDE

257876-05-4
19 suppliers
$295.00/50mL

2-(5-Chloro-2-thienyl)-5-methylpyridine

1187163-39-8
8 suppliers
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Yield:1187163-39-8 64%

Reaction Conditions:

with tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran at 20; for 24 h;Inert atmosphere;

References:

Kim, Seung-Hoi;Rieke, Reuben D. [Tetrahedron,2010,vol. 66,# 17,p. 3135 - 3146] Location in patent:scheme or table