2,5‐di(thiophen‐2‐ yl)thiazolo[5,4‐ d]thiazole synthesis
1synthesis methods
- Product Name:2,5‐di(thiophen‐2‐ yl)thiazolo[5,4‐ d]thiazole
- CAS Number:29608-87-5
- Molecular formula:C12H6N2S4
- Molecular Weight:306.45
Yield:29608-87-5 72%
Reaction Conditions:
Stage #1: thiophene-2-carbaldehyde;dithiooxamide at 150; for 0.5 h;Inert atmosphere;Microwave irradiation;
Stage #2: with chloranil in tetrahydrofuran; for 0.166667 h;Reflux;Inert atmosphere;
References:
Dessi, Alessio;Calamante, Massimo;Mordini, Alessandro;Zani, Lorenzo;Taddei, Maurizio;Reginato, Gianna [RSC Advances,2014,vol. 4,# 3,p. 1322 - 1328]