ChemicalBook CAS DataBase List 2,5-DICHLORO-2,5-DIMETHYLHEXANE

2,5-DICHLORO-2,5-DIMETHYLHEXANE synthesis

11synthesis methods

Product Name:2,5-DICHLORO-2,5-DIMETHYLHEXANE
CAS Number:6223-78-5
Molecular formula:C8H16Cl2
Molecular Weight:183.12

110-03-2 Synthesis

110-03-2
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$6.00/25g

6223-78-5
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$9.00/5g

Yield:6223-78-5 100%

Reaction Conditions:

with hydrogenchloride in water

Steps:

2,5-Dichloro-2,5-dimethylhexane (compound 2) was synthesized using a known procedure set forth in Bruson H et al., J Am Chem Soc, 62:36 (1940), whereby 50 g of 2,5-dimethylhexane-2,5-diol (compound 1 ) and 1 L of concentrated hydrochloric acid was used. Yield was measured quantitatively. Properties of compound 2 matched that reported in Bruson et al.

References:

WISCONSIN ALUMNI RESEARCH FOUNDATION WO2007/5568, 2007, A1 Location in patent:Page/Page column 10

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