2,5-DIMETHOXY-4-PYRROLIDIN-1-YL-BENZALDEHYDE synthesis
- Product Name:2,5-DIMETHOXY-4-PYRROLIDIN-1-YL-BENZALDEHYDE
- CAS Number:692775-87-4
- Molecular formula:C13H17NO3
- Molecular Weight:235.28
102-56-7
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$10.00/5g
692775-87-4
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$378.00/1g
Yield:-
Steps:
Multi-step reaction with 2 steps
1: potassium carbonate / 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide / 48 h / 120 °C
2: trichlorophosphate / 95 °C / Cooling with ice; Inert atmosphere
References:
Sarma, Monima;Chatterjee, Tanmay;Ghanta, Susanta;Das, Samar K. [Journal of Organic Chemistry,2012,vol. 77,# 1,p. 432 - 444]