2,5-dipropoxyterephthalic acid synthesis
- Product Name:2,5-dipropoxyterephthalic acid
- CAS Number:100973-03-3
- Molecular formula:C14H18O6
- Molecular Weight:282.29
Yield:100973-03-3 83%
Reaction Conditions:
Stage #1: 2,5-Dihydroxybenzol-1,4-dicarbonsaeure-dimethylester;propyl bromidewith potassium carbonate in N,N-dimethyl-formamide at 85;Schlenk technique;Williamson Ether Synthesis;
Stage #2: with sodium hydroxide in water;Reflux;
References:
Ashworth, David J.;Roseveare, Thomas M.;Schneemann, Andreas;Flint, Max;Bernáldes, Irene Dominguez;Vervoorts, Pia;Fischer, Roland A.;Brammer, Lee;Foster, Jonathan A. [Inorganic Chemistry,2019,vol. 58,# 16,p. 10837 - 10845]
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