2,6-Bis[(4S)-benzyl-2-oxazolin-2-yl]pyridine synthesis
- Product Name:2,6-Bis[(4S)-benzyl-2-oxazolin-2-yl]pyridine
- CAS Number:151670-69-8
- Molecular formula:C25H23N3O2
- Molecular Weight:397.47
499-83-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / 2 h / Reflux
2.1: triethylamine / dichloromethane / 0.17 h / Cooling with ice
2.2: 2 h / 20 °C / Reflux
3.1: potassium hydroxide / methanol / 4 h / Reflux
References:
Zhu, Yuan-Yuan;Cui, Chang;Li, Ning;Wang, Bing-Wu;Wang, Zhe-Ming;Gao, Song [European Journal of Inorganic Chemistry,2013,# 17,p. 3101 - 3111]