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ChemicalBook CAS DataBase List 2,6-di(5-bromomethylpyridine-2-yl)pyridine

2,6-di(5-bromomethylpyridine-2-yl)pyridine synthesis

5synthesis methods
2,6-di(5-methylpyridine-2-yl)pyridine

158589-14-1
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2,6-di(5-bromomethylpyridine-2-yl)pyridine

183187-82-8
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Yield:183187-82-8 56%

Reaction Conditions:

Stage #1: 5,5''-dimethyl-2,2':6',2''-terpyridinewith N-Bromosuccinimide;dibenzoyl peroxide in tetrachloromethane at 95; for 0.916667 h;
Stage #2: with diisobutylaluminium hydride in dichloromethane;Further stages.;

References:

Marquis, Annie;Smith, Virginia;Harrowfield, Jack;Lehn, Jean-Marie;Herschbach, Haiko;Sanvito, Rossella;Leize-Wagner, Emmanuelle;Van Dorsselaer, Alain [Chemistry - A European Journal,2006,vol. 12,# 21,p. 5632 - 5641]