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ChemicalBook CAS DataBase List 2,6-DI-TERT-BUTYL-4-METHYLPHENYLDIAZO ACETATE

2,6-DI-TERT-BUTYL-4-METHYLPHENYLDIAZO ACETATE synthesis

2synthesis methods
Butanoic acid, 2-diazo-3-oxo-, 2,6-bis(1,1-dimethylethyl)-4-methylphenyl ester

125641-00-1
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2,6-DI-TERT-BUTYL-4-METHYLPHENYLDIAZO ACETATE

125640-92-8
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Yield:125640-92-8 1.2 g

Reaction Conditions:

with potassium hydroxide in diethyl ether;water;acetonitrile at 20; for 4 h;Inert atmosphere;

References:

Hari, Durga Prasad;Waser, Jerome [Journal of the American Chemical Society,2017,vol. 139,# 25,p. 8420 - 8423] Location in patent:supporting information