(2,6-DibroMophenyl)Methanol synthesis

5synthesis methods

Product Name:(2,6-DibroMophenyl)Methanol
CAS Number:1013031-65-6
Molecular formula:C7H6Br2O
Molecular Weight:265.93

67713-23-9 Synthesis

67713-23-9
181 suppliers
$15.00/1g

1013031-65-6
43 suppliers
$15.00/100mg

Yield: 97%

Reaction Conditions:

with sodium tetrahydroborate in methanol at 20; for 0.5 h;Cooling with ice;

Steps:

1.B; 2.B; 3.B; 4.B B. Preparation of 2,6-dibromobenzyl alcohol
Add 2,6-dibromobenzaldehyde (25 g, 0.094 mol) to methanol (100 mL), add sodium borohydride (5.37 g, 0.142 mol) under ice bath, and react at room temperature for 30 min.After the reaction is complete, add 50 mL of water, extract with dichloromethane (50 mL×3), collect the organic phase,Drying with anhydrous sodium sulfate, filtering off the solid, evaporating the solvent under reduced pressure, beating with n-hexane (50 mL), and drying to obtain 24.3 g of 2,6-dibromobenzyl alcohol as a yellow solid with a yield of 97%.

References:

Guizhou University;Yue Yi;Zhou Zhixu;Zhao Chunshen CN108017522, 2021, B Location in patent:Paragraph 0009; 0016; 0019-0020; 0029; 0032-0033; 0042; 0045

601-84-3 Synthesis

601-84-3
131 suppliers
$11.00/100mg

1013031-65-6
43 suppliers
$15.00/100mg

References

108-36-1
449 suppliers
$10.00/1g

1013031-65-6
43 suppliers
$15.00/100mg

References

858006-31-2
9 suppliers
inquiry

1013031-65-6
43 suppliers
$15.00/100mg

References

93701-32-7
51 suppliers
$501.91/5MG

1013031-65-6
43 suppliers
$15.00/100mg

References