2,6-DICHLORO-4-PHENYL-PYRIDINE synthesis
- Product Name:2,6-DICHLORO-4-PHENYL-PYRIDINE
- CAS Number:25297-51-2
- Molecular formula:C11H7Cl2N
- Molecular Weight:224.09
2587-02-2
291 suppliers
$12.40/250mg
25297-51-2
34 suppliers
$211.21/250mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: hydrochloric acid; sodium nitrite / acetonitrile; H2O / 0.08 h / cooling
1.2: 52 percent / potassium iodide / acetonitrile; H2O
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / -78 °C
2.2: zinc chloride / tetrahydrofuran; hexane / 0.25 h
2.3: 98 percent / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran; hexane / 16 h / Heating
References:
Fang, Albert G.;Mello, Jesse V.;Finney, Nathaniel S. [Organic Letters,2003,vol. 5,# 7,p. 967 - 970]
98027-84-0
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$6.00/1g
108-86-1
499 suppliers
$10.00/5g
25297-51-2
34 suppliers
$211.21/250mg
98027-84-0
200 suppliers
$6.00/1g
28557-00-8
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25297-51-2
34 suppliers
$211.21/250mg
98027-84-0
200 suppliers
$6.00/1g
24388-23-6
208 suppliers
$6.00/5g
25297-51-2
34 suppliers
$211.21/250mg
2402-78-0
511 suppliers
$6.00/25g
591-50-4
480 suppliers
$10.00/1g
25297-51-2
34 suppliers
$211.21/250mg