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2,6-dinitro-iodobenzene synthesis

3synthesis methods
-

Yield:26516-42-7 87%

Reaction Conditions:

Stage #1: 2,6-dinitroanilinewith sulfuric acid;acetic acid;sodium nitrite for 0.5 h;Diazotization;
Stage #2: with potassium iodide in water; for 0.25 h;Heating;Iodination;

References:

Sienkowska, Monika;Benin, Vladimir;Kaszynski, Piotr [Tetrahedron,2000,vol. 56,# 2,p. 165 - 173]