ChemicalBook CAS DataBase List 2,6-Pyridinedimethanamine

2,6-Pyridinedimethanamine synthesis

12synthesis methods

Product Name:2,6-Pyridinedimethanamine
CAS Number:34984-16-2
Molecular formula:C7H11N3
Molecular Weight:137.18

3099-28-3
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$8.00/250mg

34984-16-2
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$32.00/100mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: tetrabutylammomium bromide; 18-crown-6 ether; sodium azide / dichloromethane / 17 h / 23 °C
1.2: Inert atmosphere
2.1: hydrogen; palladium 10% on activated carbon; palladium; pyrographite / ethanol / 3 h / 1520.1 Torr
2.2: Inert atmosphere

References:

Ouizem, Sabrina;Rosario-Amorin, Daniel;Dickie, Diane A.;Paine, Robert T.;De Bettencourt-Dias;Hay, Benjamin P.;Podair, Julien;Delmau, Laetitia H. [Dalton Transactions,2014,vol. 43,# 22,p. 8368 - 8386]