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2,9-Dimethyl-4,7-dihydroxy-1,10-phenanthroline synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 2 h / 110 °C
1.2: 1 h / 110 °C
2.1: diphenylether / 0.5 h / 260 °C

References:

Berrocal, José Augusto;Albano, Simone;Mandolini, Luigi;Di Stefano, Stefano [European Journal of Organic Chemistry,2015,vol. 2015,# 34,p. 7504 - 7510]