ChemicalBook CAS DataBase List 2-acetaMido-3-(2,6-difluorophenyl)propaNAic acid

2-acetaMido-3-(2,6-difluorophenyl)propaNAic acid synthesis

2synthesis methods

Product Name:2-acetaMido-3-(2,6-difluorophenyl)propaNAic acid
CAS Number:266360-50-3
Molecular formula:C11H11F2NO3
Molecular Weight:243.21

85118-00-9 Synthesis

85118-00-9
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2-acetaMido-3-(2,6-difluorophenyl)propaNAic acid

266360-50-3
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: 90 percent / NaOEt / ethanol / 2 h / Heating
2: 2M NaOH / methanol; H₂O / 3 h / 40 °C
3: 92 percent / p-xylene / 2 h / Heating

References:

Fujita, Tsugumi;Nose, Takeru;Matsushima, Ayami;Okada, Kazushi;Asai, Daisuke;Yamauchi, Yasuko;Shirasu, Naoto;Honda, Takeshi;Shigehiro, Daiki;Shimohigashi, Yasuyuki [Tetrahedron Letters,2000,vol. 41,# 6,p. 923 - 927]

Propanedioic acid, 2-(acetylamino)-2-[(2,6-difluorophenyl)methyl]-, 1,3-diethyl ester

266360-45-6
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266360-50-3
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References