2-ACETOXY-PYRIDINE synthesis
- Product Name:2-ACETOXY-PYRIDINE
- CAS Number:3847-19-6
- Molecular formula:C7H7NO2
- Molecular Weight:137.14
Yield:3847-19-6 90%
Reaction Conditions:
Stage #1: 2-hydroxypyridinwith tetra(n-butyl)ammonium hydrogensulfate;sodium hydroxide in dichloromethane at 20; for 0.0833333 h;
Stage #2: acetyl chloride in dichloromethane at 20;
References:
Xu, Guangyang;Chen, Ping;Liu, Pei;Tang, Shengbiao;Zhang, Xinhao;Sun, Jiangtao [Angewandte Chemie - International Edition,2019,vol. 58,# 7,p. 1980 - 1984][Angew. Chem.,2019,vol. 131,# 7,p. 2002 - 2006,5] Location in patent:supporting information
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